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Everything You need to Know about ASTM B166

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Overview

ASTM B166 is a standard for nickel alloy / superalloy bar and rod. It includes many very common alloy materials. In this article, we will extract the noteworthy requirements in ASTM B166 for you in detail, which will allow you to better control the quality in product procurement and inspection.

Grades & Chemical Composition

Grades

The main scope of ASTM B166 is nickel-chromium-iron alloys. Among them, the common materials are: Inconel 600 (UNS N06600), Inconel 601 (UNS N06601), Inconel 602CA (UNS N06025), Inconel 690 (UNS N06690) and Inconel 693 (UNS N06693). The two compositions of nickel and chromium bring resistance to various corrosions to the alloy. Additionally, the standard includes a nickel-chromium-cobalt-molybdenum alloy, Inconel 617 (UNS N06617). In this alloy, cobalt and molybdenum elements improve the solid solution strengthening effect of the alloy, allowing the alloy to obtain higher strength.

Chemical Composition

Inconel 600 (UNS N06600)

600

Si

C

Mn

Cu

Fe

Cr

Ni

Inconel 601 (UNS N06601)

601

Si

C

Mn

Al

Cu

Fe

Cr

Ni

Inconel 602CA (UNS N06025)

602CA

Si

C

Al

Y

Fe

Cr

Ni

Inconel 617 (UNS N06617)

617

Si

C

Mn

Al

Ti

Cu

Co

Mo

Fe

Cr

Ni

Inconel 690 (UNS N06690)

690

Si

Cu

Fe

Cr

Ni

Inconel 693 (UNS N06693)

693

Si

C

Mn

Al

Ti

Cu

Nb

Fe

Cr

Ni

The supplier shall perform a chemical analysis of the alloy in accordance with ASTM B880.

Product Properties

Products in ASTM B166

ASTM B166 mainly includes three products: rod, bar and wire.

Among them, Bars are divided into round bar, square bar, flat bar and hexagon bar according to the cross-sectional shape. Large size bars are generally produced by hot rolling process. Smaller sizes of bars are produced by cold drawing. Among them, the small size round bar is also called rod.

Wires are generally produced by cold drawing. Smaller in size and continuous in length. Wires can more finely control the properties of the alloy through the combination of cold drawing and heat treatment.

Mechanical Properties

Mechanical Properties of Rods and Bars
Condition and Diameter or Distance
Between Parallel Surfaces, in. (mm)
Tensile Strength,
min, psi (MPa)
Yield Strength (0.2 %
offset), min, psi (MPa)
Elongation in 2 in. or
50 mm or 4D, min,%
Inconel 600 (UNS N06600)
Cold-worked (as worked):
Rounds, Under 1/2 (12.7) 120 000 (825) 90 000 (620) 7
Rounds, 1/2 to 1 (12.7 to 25.4), incl 110 000 (760) 85 000 (585) 10
Rounds, Over 1 to 2-1/2 (25.4 to 63.5), incl 105 000 (725) 80 000 (550) 12
Squares, hexagons, and rectangles,
1/4 (6.4) and under
100 000 (690) 80 000 (550) 5
Squares, hexagons, and rectangles,
Over 1/4 to 1/2 (6.4 to 12.7), excl
95 000 (655) 70 000 (480) 7
Hot worked (as worked):
Rounds, 1/4 to 1/2 (6.4 to 12.7), incl 95 000 (655) 45 000 (310) 20
Rounds, Over 1/2 to 3 (12.7 to 76.2), incl 90 000 (620) 40 000 (275) 25
Rounds, Over 3 (76.2) 85 000 (585) 35 000 (240) 30
Squares, hexagons, and rectangles, All sizes 85 000 (585) 35 000 (240) 20
Cold-worked (annealed) or hot-worked (annealed):
Rods and bars, all sizes 80 000 (550) 35 000 (240) 30
Inconel 601 (UNS N06601)
Cold-worked (annealed) or hot-worked (annealed):
All products, all sizes 80 000 (550) 30 000 (205) 30
Inconel 617 (UNS N06617)
Cold-worked (annealed) or hot-worked (annealed):
All products, all sizes 95 000 (655) 35 000 (240) 35
Inconel 690 (UNS N06690)
Cold-worked (as worked):
Rounds, Under 1/2 (12.7) 120 000 (825) 90 000 (620) 7
Rounds, 1/2 to 1 (12.7 to 25.4), incl 110 000 (760) 85 000 (585) 10
Rounds, Over 1 to 2-1/2 (25.4 to 63.5), incl 105 000 (725) 80 000 (550) 12
Squares, hexagons, and rectangles,
1/4 (6.4) and under
100 000 (690) 80 000 (550) 5
Squares, hexagons, and rectangles,
Over 1/4 to 1/2 (6.4 to 12.7), excl
95 000 (655) 70 000 (480) 7
Hot worked (as worked):
Rounds, 1/4 to 1/2 (6.4 to 12.7), incl 95 000 (655) 45 000 (310) 20
Rounds, Over 1/2 to 3 (12.7 to 76.2), incl 90 000 (620) 40 000 (275) 25
Rounds, Over 3 (76.2) 85 000 (585) 35 000 (240) 30
Squares, hexagons, and rectangles,
All sizes
85 000 (585) 35 000 (240) 20
Cold-worked (annealed) or hot-worked (annealed):
Rods and bars, all sizes 85 000 (586) 35 000 (240) 30
Inconel 693 (UNS N06693)
Cold-worked (annealed) or hot-worked (annealed):
Rods and bars, all sizes 100 000 (690) 50 000 (345) 30
UNS N06603
Cold-worked (annealed) or hot-worked (annealed):
All products, all sizes 94 000 (650) 43 000 (300) 25
Inconel 602CA (UNS N06025)
Cold-worked (annealed) or hot-worked (annealed):
All products, all sizes 98 000 (680) 39 000 (270) 30
UNS N06045
Cold-worked (annealed) or hot-worked (annealed):
All products, all sizes 90 000 (620) 35 000 (240) 35
Hot-worked (Annealed):
Rods and bars, all sizes 75 000 (517) 30 000 (207) 30
UNS N06696
Cold-worked (annealed and water quenched) or
hot-worked (annealed and water quenched):
All products, all sizes 85 000 (586) 35 000 (240) 30
Mechanical Properties of Cold-Worked Wire in Coil (Alloys N06600 and N06690 Only)
Condition and Size, in, (mm) Tensile Strength, psi (MPa) Wrapping Test
Min Max
Annealed The wire shall be wrapped eight consecutive turns in a closed helix (pitch approximately equal to the diameter of the wire) around a mandrel as follows:
(1) For all annealed and regular temper wire and for spring temper wire 0.229 in. (5.82 mm) and less: Same as diameter of wire.
(2) For spring temper wire over 0.229 in. (5.82 mm): Twice the diameter of wire.
The wire shall withstand the wrapping test without fracture or development of a pebbled or orange-peel surface.
Under 0.032 (0.81) 80 000 (552) 115 000 (793)
0.032 (0.81) and over 80 000 (552) 105 000 (724)
Cold-worked, regular temper
All sizes 120 000 (827) ...
Cold-worked, spring temper ... 165 000 (1138)
Up to 0.057 (1.45), incl 185 000 (1276) ...
Over 0.057 (1.45) to 0.114 (2.90), incl 175 000 (1207) ...
Over 0.114 (2.90) to 0.229 (5.82), incl 170 000 (1172) ...
Over 0.229 (5.82) to 0.329 (8.36), incl 165 000 (1138) ...
Over 0.329 (8.36) to 0.375 (9.53), incl 160 000 (1103) ...
Over 0.375 (9.53) to 0.500 (12.7), incl 155 000 (1069) ...
Over 0.500 (12.7) to 0.563 (14.3), incl 140 000 (965) ...

Delivery State

For bars and rods, most alloys are delivered in the annealed condition. The alloy in this state has lower strength but better toughness.

For Inconel 600, Inconel 690 and Inconel 693, the standard also specifies the status of hot-worked and cold worked. These two states retain more work hardening, giving the material higher strength. Among them, the strength of the cold-worked state material can reach the maximum.

For wires, the standard specifies the different states of Inconel 600 and Inconel 690. Like bars, wires also have annealed and cold-worked states. In addition, wires also have the status of spring temper. This product is also known as spring wire. It is mainly used to make springs and has extreme tensile properties.

Other Information

Dimension

The standard specifies the dimensional tolerances of hot-rolled bars, cold-rolled bars and wires respectively. Please refer to the table below:

Permissible Variations in Diameter or Distance
Between Parallel Surfaces of Cold-Worked Rod and Bar
Specified Thickness,
in. (mm)
Permissible Variations in Thickness,
in. (mm)
+ -
Rounds:
1/16 (1.6) to 3/16 (4.8), excl 0 0.002 (0.05)
3/16 (4.8) to 1/2 (12.7), excl 0 0.003 (0.08)
1/2 (12.7) to 15/16 (23.8), incl 0.001 (0.03) 0.002 (0.05)
over 15/16 (23.8) to 1-15/16 (49.2), incl 0.0015 (0.04) 0.003 (0.08)
over 1-15/16 (49.2) to 2-1/2 (63.5), incl 0.002 (0.05) 0.004 (0.10)
Hexagons, squares, rectangles:
1/2 (12.7) and less 0 0.004 (0.10)
over 1/2 (12.7) to 7/8 (22.2), incl 0 0.005 (0.13)
over 7/8 (22.2) to 1-1/4 (31.8), incl 0 0.007 (0.18)
over 1-1/4 (31.8) to 2 (50.8), incl 0 0.009 (0.23)
Permissible Variations in Diameter or Distance
Between Parallel Surfaces of Hot-Worked Rod and Bar
Specified Thickness,
in. (mm)
Permissible Variations in Thickness,
in. (mm)
+ -
Rod and bar, hot-worked:
1 (25.4) and under 0.016 (0.41) 0.016 (0.41)
over 1 (25.4) to 2 (50.8), incl 0.031 (0.79) 0.016 (0.41)
over 2 (50.8) to 4 (101.6), incl 0.047 (1.19) 0.031 (0.79)
over 4 (101.6) 0.125 (3.18) 0.063 (1.60)
Rod, rough-turned or ground:
under 1 (25.4) 0.005 (0.13) 0.005 (0.13)
1 (25.4) and over 0.031 (0.79) 0
Forging quality rod:
Under 1 (25.4) 0.005 (0.13) 0.005 (0.13)
1 (25.4) and over 0.031 (0.79) 0
Permissible Variations in Diameter of Cold-Worked Wire
Diameter, in. (mm) Permissible Variations, in.
(mm)
+ or −
Up to 0.0044 (0.112), incl 0.0002 (0.005)
Over 0.0044 (0.112) to 0.0079 (0.201), incl 0.00025 (0.006)
Over 0.0079 (0.201) to 0.0149 (0.378), incl 0.0003 (0.008)
Over 0.0149 (0.378) to 0.0199 (0.505), incl 0.0004 (0.010)
Over 0.0199 (0.505) to 0.031 (0.79), incl 0.0005 (0.013)
Over 0.031 (0.79) to 0.045 (1.14), incl 0.0006 (0.015)
Over 0.045 (1.14) to 0.079 (2.01), incl 0.0007 (0.018)
Over 0.079 (2.01) to 0.1875 (4.76), incl 0.001 (0.025)
Over 0.1875 (4.76) to 0.3125 (7.93), incl 0.002 (0.051)
Over 0.3125 (7.93) to 0.563 (14.3), incl 0.003 (0.076)
Permissible Variations in Length of Rods and Bars
Random mill lengths:
Hot-worked 6 to 24 ft (1.83 to 7.31 m) long with not more than 25 weight % between 6 and 9 ft (1.83 and 2.74 m).
Cold-worked 6 to 20 ft (1.83 to 6.1 m) long with not more than 25 weight % between 6 and 10 ft (1.83 and 3.05 m).
Multiple lengths Furnished in multiples of a specified unit length, within the length limits indicated above. For each multiple, an allowance of 1/4 in. (6.4 mm) will be made for cutting, unless otherwise specified. At the manufacturer’s option, individual specified unit lengths may be furnished.
Nominal lengths Specified nominal lengths having a range of not less than 2 ft (610 mm) with no short lengths allowed.
Cut lengths A specified length to which all rods and bars will be cut with a permissible variation of plus 1/8 in. (3.2 mm), minus 0 for sizes 8 in. (203 mm) and less in diameter or distance between parallel surfaces. For larger sizes, the permissible variation shall be + 1/4 in. (6.4 mm), − 0.

Straightness

ASTM B166 stipulates the allowable range of straightness for hot-rolled bars and cold-rolled bars respectively. The supplier shall straighten the material in strict accordance with the requirements.

Permissible Variations in Straightness of Cold-Worked Rods and Bars
Specified Diameter or Distance
Between Parallel Surfaces, in. (mm)
Permissible Variations
in Lengths Indicated, in. (mm)
Rounds: Depth of Chord:
1/2 (12.7) to 2 1/2 (63.5), incl 0.030 (0.76) per ft (305 mm) of length
Hexagons, squares, rectangles:
1/2 (12.7) to 2 (50.8), incl 0.030 (0.76) per ft (305 mm) of length
Permissible Variations in Straightness of Hot-Worked Rods and Bars
Finish Permissible
Variations,
in./ft (mm/m)
Rods and bars, hot-worked 0.050 (4.2)
Rounds hot-worked, rough-ground, or rough-turned 0.050 (4.2)

Certification

The supplier shall provide the material test certificate corresponding to the material when delivering the goods. The certificate should list customer information, supplier information, standards, heat number, product form, delivery status, size, chemical composition, mechanical properties and other necessary information in detail.

Conclusion

ASTM B166 mainly contains some commonly used nickel-chromium-iron alloys and nickel-chromium-cobalt-molybdenum alloys. Most of the alloys in the standard have excellent corrosion resistance. The products in ASTM B166 are mainly bars, rods and wires. For some grades, different delivery states are specified in the standard, please fully confirm with the supplier before placing an order.

We produce corresponding products strictly according to the standard of ASTM B166. If you have needs, please do not hesitate to contact us.

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